ORDER OF THE MINISTRY OF AGRARIAN POLICY OF UKRAINE

of April 13, 2009 No. 264

About approval of the Instruction for acceptance, storage, leave, transportation and accounting of ethyl alcohol

According to the Regulations on the Ministry of agrarian policy of Ukraine approved by the resolution of the Cabinet of Ministers of Ukraine of November 1, 2006 N 1541, and for the purpose of strengthening of the state control of implementation of processes of acceptance, storage, leave, transportation and accounting of ethyl alcohol I ORDER:

1. Approve the Instruction for acceptance, storage, leave, transportation and accounting of ethyl alcohol it (is applied).

2. Consider the "Instruction for the acceptance, storage, leave, transportation and accounting of ethyl alcohol" approved by the Ministry of the Food Industry of the USSR on September 25, 1985 which is not applied in the territory of Ukraine.

3. To department of the food industry (Kishchak Yu. P.) provide submission of this order in accordance with the established procedure on state registration in the Ministry of Justice of Ukraine.

4. This order becomes effective from the date of its official publication.

5. To impose control over the implementation of this order on the deputy minister Demchak I. M.

 

Approved by the Order of the Ministry of agrarian policy of Ukraine 13.04.2009 No. 264

Instruction for acceptance, storage, leave, transportation and accounting of ethyl alcohol

I. General provisions

1. This Instruction extends to all types, grades and brands of ethyl alcohol, aqueous-alcoholic solutions and products of bragorektifikation (further - alcohol).

2. This Instruction establishes single requirements to accounting, storage, leave, acceptance and transportation of alcohol by subjects of managing (further - the company) which perform such activities and use alcohol in engineering procedure.

3. Accounting of alcohol perform in decalitres of anhydrous alcohol (further - gave B. page) at temperature of 20 hail. With to within one cell gave B. page. Thousand shares, less 0,005, discard, and accept 0,005 for one 100-th gave B. page more.

4. For calculation of amount of anhydrous alcohol it is necessary to measure the following parameters:

the total amount of alcohol in decalitres (further - gave) or the mass of alcohol in kilograms;

average temperature of the measured alcohol amount in case of measurement by volume method (measuring tanks) or the actual temperature in the reservoir by alcohol measurement by roulette with lot according to GOST 7502 "Roulettes measuring metal. Specifications" or metrshtoky (basting) during hail. With;

volume fraction of ethyl alcohol at temperature of 20 hail. With, as a percentage (%), in the measured amount (weight).

5. It is possible to take measurement means of the measuring equipment which are entered in the State register of means of the measuring equipment and have the existing certificates on checking granted by specially authorized central executive body in the field of metrology (further - TsOVM).

6. The amount of alcohol is measured by metal technical measuring tanks of the I class in reservoir from 0,5 gave to 5000 gave according to GOST 13844 "Measuring tanks metal technical. Methods and means of checking" (further - GOST 13844) which underwent at the scheduled time the state checking have seals or brands of the state verificator and the certificate on their checking, and laboratory glass measuring glassware according to GOST 1770 "Ware measuring laboratory glass. Cylinders, beakers, flasks, test tubes. General specifications" (further - GOST 1770).

In reservoir more than 50 gave measuring tanks shall be stationary. The state checking of all measuring tanks which are operated by the company (including spirtobaza) is carried out at the same time same measuring tanks by representatives of TsOVM according to the current legislation and according to GOST 13844.

Checking is carried out surely in the presence of the chief of production (technological) laboratory and the responsible person working with these measuring tanks.

Covers of measuring tanks after check are sealed up by the representative of TsOVM which carried out their checking in the presence of the above-stated officials.

7. The mass of alcohol is measured by scales for static weighing according to GOST 29329 "By scales for static weighing. General technical requirements". The error of weighing of scales during operation at the company shall be no more, than:

+-1 division of scale during weighing of weight to 2000 testing prices of divisions;

+-2 divisions of scale during weighing of weight more than 2000 testing prices of divisions.

The mass of alcohol is determined as weight difference gross also by tare masses.

Weight gross and tare mass which weigh shall correspond to the range of measurement of scales. Weighing of loads which mass does not correspond to the measurement range established for scales, inadmissibly. The choice of the range of measurement of scales is performed proceeding from condition of ensuring weighing of the maximum and minimum weight with which plan to work at this company. For reduction of influence of the environment by error of measurements weight devices protect from wind and rainfall.

The size of result of weighing is rounded to the category of size of absolute error.

8. During measurement of amount or mass of alcohol select average test from this batch of alcohol according to DSTU 5043 "Ethyl alcohol and alcohol-containing liquids. Methods of collecting of tests" (to daleedst 5043) and DSTU 4181 "Ethyl alcohol the rectified and ethyl alcohol - raw. Acceptance procedures and test methods" (further - DSTU 4181).

9. The volume fraction of ethyl alcohol (fortress) in this test is measured according to GOST 3639 "By solutions aqueous-alcoholic. Methods of determination of concentration of ethyl alcohol", DSTU 4181 glass areometers for alcohol of the ASP-1 or ASP-2 type according to GOST 18481 "Areometers and cylinders glass. Specifications" with the price of division the % there is no more 0, about. or automatic analyzers of density according to the existing regulating documentation. Temperature of average test of alcohol is taken the liquid glass thermometer according to GOST 28498 "By thermometers liquid glass. General technical requirements. Test methods" with the price of division of 0,1 hail. With and the measurement range from 0 to 50 hail. With or other thermometers according to the existing regulating documentation. It is allowed to apply other means of the measuring equipment with similar technical characteristics.

The measured size of volume fraction of ethyl alcohol lead the 20th hail to temperature. C. Calculations perform with use of tables

1.1 - 1.3 handbook "Tables spirtometrichesky. Handbook" / V. K. Yanchevsky, S. T. Oliynichuk, Z. D. Kravchuk, V. P. Kovalchuk, V. N. Mikhaylo. - Ukrniispirtbioprod, 2002/(further - Tables).

10. Amount of anhydrous alcohol at temperature of 20 hail. With, V, 20 gave B. page which contains in the measured alcohol amount, calculate by formula:

where: V - amount of the measured alcohol at average temperature in t measuring tanks taking into account the amendment on volume expansion of measuring tanks from temperature estimated according to the Correction table on volume expansion of metal technical measuring tanks of the I class during measurement of amount of alcohol (appendix 1)/further - the Correction table/;

n - multiplier for calculation of amount of anhydrous alcohol, which

20 contains in alcohol amount at temperature of 20 hail. With, the hail determined by spirtometrichesky tables 2.1-2.3 of Tables depending on volume fraction of ethyl alcohol at temperature of 20. With in average test and average temperature of the measured alcohol amount.

11. Amount of anhydrous alcohol at temperature of 20 hail. With, V, 20 gave B. page which contains in certain mass of alcohol, calculate by formula:

where: M - the mass of the weighed alcohol, kg;

n - multiplier for calculation of amount of anhydrous alcohol, which

20 contains in alcohol amount at temperature of 20 hail. With, determined by spirtometrichesky tables 2.1 - 2.3 Tables depending on volume fraction of ethyl alcohol at temperature of 20 hail. With in average test and average temperature of the measured alcohol amount;

(ро) - alcohol density at temperature of 20 hail. With in average 20th test, determined by spirtometrichesky table 3.1 of Tables on volume fraction of ethyl alcohol at temperature of 20 hail. With in average test, kg / куб.дм;

0,0012 - air density under normal conditions, kg / куб.дм;

10 - the conversion factor of cubic dm in gave.

12. Amount of anhydrous alcohol at temperature of 20 hail. With, V, 20 gave B. page, it is possible to determine the omission of alcohol through means of electronic accounting with automatic receipt of result of measurement on the display of the device.

On the display of the device such parameters of results of measurement of batch of alcohol shall be specified:

total amount, gave, or the weight, kg;

average temperature, hail. With;

average value of volume fraction of ethyl alcohol at temperature of 20 hail. With as a percentage in the measured amount.;

the amount of anhydrous alcohol, gave B. page.

Means of electronic accounting shall be certified in Ukraine according to the current legislation and have relative error of measurement of anhydrous alcohol no more +-% 0,2.

These means of electronic accounting can be united in measuring complexes of automation of engineering procedures which perform automatic measuring off of the set amount of anhydrous alcohol with the corresponding automatic turning on and switching off of pumps, accomplishment of the corresponding transactions with the locking and adjusting equipment. Such measuring complexes shall guarantee storage of information on results of measurement and its protection against corrections and modification.

13. Means of electronic accounting which are applied in technology of measurement of amount of alcohol shall have the existing certificates on checking granted by bodies of TsOVM, have seals according to the scheme of sealing which excludes possibility of unauthorized intervention in operation of the metering device.

14. Alcohol is considered by the company in quantity which is actually established by the Act of production of alcohol, products of bragorektifikation and their transfer in spirtokhranilishche in the P-18 form (appendix 2)/further - the P-18 form/, or specified in commodity-transport delivery note on movement of ethyl alcohol in the N 1-TH/alcohol form/, Ukraine approved by the order of the Ministry of Transport and Communications of 28.04.2005 N 154 "About approval of the Instruction about application of forms of commodity-transport delivery notes on movement of ethyl alcohol, high-octane oxygencontaining impurity and alcoholic beverages, forms of commodity-transport delivery notes on movement of ethyl alcohol, high-octane oxygencontaining impurity and alcoholic beverages" registered in the Ministry of Justice of Ukraine 28.07.2005 for N 817/11097 (further - the N 1-TH/alcohol form/).

15. The P-18 form is intended for accounting of daily production of ethyl alcohol - raw and products of bragorektifikation on counters of control spirtoizmeritelny devices and on plum during their transfer in spirtokhranilishche. The statement is drawn up by the production manager in duplicate: the original is given in accounts department, and the copy remains in the workshop.

In case of measurement of amount of alcohol by volume method in the Section II of the P-18 form Items 2 and 10 do not fill.

In case of measurement of amount of alcohol do not fill with weight method in the Section II of the P-18 form Items 1 - 4 and 6.

In case of measurement of amount of alcohol fill with means of electronic accounting in the Section II of the P-18 form Items 1, 9 and 12.

The reverse side of the act is filled in case of measurement of amount of alcohol with volume method.

16. Control of amounts of the made alcohol is exercised spirtoizmeritelny devices or means of electronic accounting (further - automatic accounting). Results of automatic accounting fix in register of production of alcohol on indicators of counters of control spirtoizmeritelny devices in the P-21 form (appendix 3)/further - the P-21/form. Sheets of the magazine shall be numbered, strung together, under seal and certified by the signature of the head and chief accountant of the manufacturing company.

17. Write-off of losses of alcohol in storage time and transportations within regulations of natural losses is carried out according to the written order of the director.

Maximum permissible natural losses of alcohol calculate according to Regulations of natural losses of alcohol in case of storage, movement, transportation by the railway, water and road transport approved by Gosspetsmonopoliya's order of Ukraine of 10.02.2000 of N 14, registered in the Ministry of Justice of Ukraine 29.02.2000 for N111/4332 (further - Regulations of natural losses). Regulations of natural losses apply only in case of identification of the actual losses of alcohol in storage time, movement and transportation.

II. Procedure for leave of alcohol

1. General requirements to alcohol leave

1. Leave of alcohol is performed in lots. The amount of alcohol of one name, one shipping date which is drawn up by one quality certificate and one accompanying document (the N 1-TH/spirt form/) or the rail waybill is considered batch.

2. Alcohol releases person, materially responsible for its safety, with obligatory participation of the representative of production laboratory of the company who together with the responsible person provides correctness of sampling, determination of volume fraction of alcohol in case of the 20th hail. With and average temperature in measuring tanks.

3. Leave of alcohol is performed by measurement of amount of alcohol in batch one of the methods given in Items 6-12 of the Section I of the Instruction (the omission through measuring tanks or electronic means of accounting or weighing on scales). Results of measurement are the amount or mass of alcohol, its average temperature and fortress. Results of further calculations are volume fraction of ethyl alcohol at temperature of 20 hail. With and amount of anhydrous alcohol in batch at temperature of 20 hail. C. The resulting effect and intermediate results of calculations are written down in register of otmer of alcohol in the P-23 form (appendix 4)/further - the P-23/form.

The magazine in the P-23 form fills the responsible person of spirtokhranilishch (warehouse) during each acceptance and leave (shipment) of alcohol which perform based on the relevant documents.

In case of alcohol measurement by volume method (the omission through measuring tanks) in the magazine write down everyone died off alcohol immediately after selection of the corresponding part of average test, determination of temperature in measuring tank and opening of armature on discharge of alcohol from measuring tank. After the termination of the last otmer count total quantity of alcohol in decalitres; remove the average temperature of alcohol in measuring tanks; on the average temperature of alcohol according to the Correction table (appendix 1) enter the amendment on volume expansion of measuring tanks and determine multiplier and calculate amount of anhydrous alcohol (gave B. page).

In case of measurement of amount of alcohol by volume method Items 2 and 10 of the P-23 form do not fill.

In case of measurement of amount of alcohol do not fill with weight method Items 1, of the 3 - 5 and 8 P-23 form.

In case of measurement of amount of alcohol fill with means of electronic accounting Items 1, of the 9 and 12 P-23 form.

The amount of alcohol which is selected during cleaning of the cistern car is written down in the magazine separately with the mark "cleaning".

Each transaction during otmer of alcohol is fastened with the corresponding signatures.

In case of carrying out inventory count of alcohol by volume method (the omission through measuring tanks) (on the separate page) the made otmer of alcohol, and also all other indicators which are fixed by the commission, quantities of decalitres of anhydrous alcohol, necessary for determination, write down in the magazine.

These data are confirmed with signatures by all members of inventory-taking group.

4. In case of measurement of amount of alcohol in batch measuring tanks partial plums and dolivaniye of measuring tank are admissible only for two last measurements of batch of alcohol vertical cylindrical measuring tanks. Average test of alcohol from this batch is created, selecting alcohol from each measuring tank it is pro rata to its reservoir through three specially established in crane measuring tank. Average test select according to DSTU 5043, amount of which there shall be at least than 1 cubic dm.

During measurement fix alcohol amount in each measuring tank and alcohol temperature in measuring tank, hail. With which measure by the thermometers established in the middle of frontal part of measuring tank and volume fraction of ethyl alcohol at temperature of 20 hail. With as a percentage in the measured amount. The total amount of alcohol is determined as the amount of the amounts measured by measuring tanks. If in case of measurement alcohol temperature in measuring tank differs from the 20th hail. With, the amendment on volume expansion of measuring tank irrespective of the variation sizes from normal temperature according to the Correction table is applied (appendix 1). The amendment is made separately to all documents for alcohol leave. Average temperature of batch of alcohol is determined as arithmetic-mean (measuring tanks of one reservoir) or srednedinamichesky (measuring tanks of different reservoir) by values of temperatures taken in measuring tanks. The amount of anhydrous alcohol is determined by formula (1), the Instruction provided in Item 10 of the Section I. Examples of calculations in case of measurement of anhydrous alcohol in batches are given in appendix 5.

5. In case of measurement of amount of alcohol in batch weight method all amount of alcohol in batch is repumped in stationary or portable container which is weighed on the corresponding scales. From the mass of alcohol with container (gross) subtract tare mass and receive the mass of batch of alcohol (net). Weighing can be performed for one or several times. Volume fraction of ethyl alcohol at temperature of 20 hail. With determine in the average test which is selected from that reservoir from which ship alcohol batch, or from the consumer's container, or from container in which weigh alcohol batch. Average test is selected according to DSTU 5043. The amount of anhydrous alcohol is determined by formula (2), the Instruction provided in Item 11 of the Section I.

6. In case of alcohol measurement by electronic means of accounting it is necessary to pass through the called means all amount of alcohol in batch. Results of measurement receive automatically on the display of electronic means of accounting.

In case of doubts concerning correctness of operation of metering devices volume fraction of ethyl alcohol at temperature of 20 hail. With in addition control in the average test which is selected from the reservoir from which ship, or from container in which merge alcohol batch, according to DSTU 5043.

7. Leave of alcohol in the contaminated and defective container is prohibited.

2. Procedure for leave of alcohol from production in spirtokhranilishche

1. Vacation (transfer) of alcohol from production in spirtokhranilishche is spent daily. After days off and holidays in spirtokhranilishche it is possible to perform leave of alcohol from production once in two three days in the presence in spirtopriyemny department of reservoirs of sufficient amount.

2. Prior to leave of alcohol from production in spirtokhranilishche employee of laboratory performs selection of average test from all amount of the alcohol which is subject to transfer. Test is selected according to DSTU 5043. By results of alcohol test conformity testing to requirements of DSTU 4221 "The ethyl alcohol rectified. Specifications" (further - DSTU 4221) determine grade of the made alcohol batch.

In case of use of measuring tanks, general for spirtopriyemny department and spirtokhranilishch, and the corresponding technical capabilities alcohol leave implementation to the consumer directly from spirtopriyemny department, in the presence of the job specification and the written order of the director on leave is allowed. Accounting of leave of alcohol is performed with the corresponding display in alcohol registers in spirtokhranilishche in the P-20 form (appendix 6)/further - the P-20 form/, accounting of alcohol in reservoirs in the P-22 form (appendix 7)/further - the P-22/form and in the P-23 form.

3. Prior to alcohol leave the bureaucrat of bragorektifikatsionny installation temporarily closes selection of alcohol from installation and after the termination of intake of alcohol in the control spirtoizmeritelny device or electronic means of accounting of production of alcohol writes down device counter indicators in the magazine in the P-21 form. These indicators of the device and indicators which were received before the previous transfer of alcohol from spirtopriyemny department in spirtokhranilishche fix also in the act in the P-18 form. Results of measurement of amount of alcohol and amount of anhydrous alcohol counters of control spirtoizmeritelny devices or electronic means of accounting fix in the act separately for each counter.

Fixing of indicators of control spirtoizmeritelny devices or electronic means of accounting is performed for the beginning of first shift of days, except cases of business necessity of additional urgent check of work of the specified means.

After record of indicators of the counter the bureaucrat blocks the crane on communication of supply of alcohol after the spirtoizmeritelny device in the completed collection of alcohol and opens the crane of supply of alcohol on the collection of spirtopriyemny department, free from alcohol, resumes selection of alcohol from installation.

It is forbidden to carry out fixation of indicators of metering devices during alcohol selection.

All alcohol made at the time of fixation of indicators of the counter of the spirtoizmeritelny device shall be measured and transferred from production in spirtokhranilishche on the same day.

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